Synthesis and characterization of quaternary alloys CuTaAlSe3 AND CuTaGaSe3

Authors

DOI:

https://doi.org/10.13140/RG.2.2.21301.83684

Keywords:

Alloys, x-ray diffraction, differential thermal analysis

Abstract

The ingots of CuTaAlSe3 and CuTaGaSe3 were synthesized using the melt and annealing technique. X-Ray Diffraction (XRD) and Differential Thermal Analysis (DTA) techniques were used for characterization of the alloy. The analysis of the diffraction pattern indicates that both samples are composed by two phases; the mean phase indexes as a hexagonal structure, whereas the secondary phase indexes as a tetragonal chalcopyrite-like structure. From the shape of the DTA peaks for the CuTaAlSe3 and CuTaGaSe3 alloys, was deduced that the melting is incongruent for both materials, value of ~1348K and ~1235K, respectively.

 

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Author Biographies

Marcos Antonio Muñoz Pinto, Universidad Centroccidental Lisandro Alvarado, Venezuela

Doctor. Profesor Investigador en la Universidad Centroccidental Lisandro Alvarado, Venezuela. Correo: mamp25571@gmail.com  Perfil en Google Scholar

Sonia del Valle Durán Piña, Universidad Centroccidental Lisandro Alvarado, Venezuela

Doctora. Profesora Investigadora en la Universidad Centroccidental Lisandro Alvarado, Venezuela. Correo: spina9730@gmail.com.  Perfil en Google Scholar.

Pedro José Grima Gallardo, Universidad de Los Andes, Venezuela

Doctor. Profesor e Investigador. Centro Nacional de Tecnología Óptica (CNTO). Centro de Investigaciones de Astronomía (CIDA). Centro de Estudios en Semiconductores (CES). Faccultad de Ciencias, Universidad de Los Andes (ULA), Mérida. Venezuela.

Gerzon Eusebio Delgado Arciniegas, Universidad de Los Andes, Venezuela

Licenciado en Química. Magister en Química Aplicada, Mención Estudio de Materiales. Doctor en Química Aplicada. Profesor e investigador Laboratorio de Cristalografía, Departamento de Química, Facultad de Ciencias, Universidad de Los Andes (ULA), Mérida, Venezuela. Correo electrónico: gerson@ula.ve.
Perfil de Google Scholar

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Published

2019-06-30

How to Cite

[1]
M. A. Muñoz Pinto, S. del V. Durán Piña, P. J. Grima Gallardo, and G. E. Delgado Arciniegas, “Synthesis and characterization of quaternary alloys CuTaAlSe3 AND CuTaGaSe3”, Publ.Cienc.Tecnol, vol. 13, no. 1, pp. 4-14, Jun. 2019.

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Section

Research Article