Determination of total phenol derivatives obtained from lignin black liquor as alternative to production

Authors

  • María José López Villalobos Mediwork Servicios C.A
  • Irama Isabel Piña Sáenz Universidad del Zulia, Venezuela
  • Yakelin Abou Masoud Laboratorio Clinico Bonaiuto, Venezuela
  • Fredy José Ysambertt Universidad del Zulia, Venezuela

Keywords:

Lignin, waste, precipitation, phenols, antioxidants

Abstract

Lignin is an industrial waste being worthless in papermaking byproduct of black liquor obtained from the pulping process in some Venezuelan plants. The black liquor is obtained from the Kraft pulping process to extract lignin sulphite by acid precipitation and quantify the amount of total phenols in such lignin products used in this study. Spectrophotometry Molecular absorption in the UV-Visible and Infrared Spectroscopy (FTIR) region were used to carry out these study techniques. The products obtained in the study had the same signs than commercial lignin (LA), along with the extracted lignin present little degradation HCl, confirmed by infrared spectra. Also, the amount of total phenols was quantified in derivative lignin obtained using the Folin-Ciocalteu. In the sulphite process extracted lignin with acetic acid derivative contains more phenols, and in the Kraft process, the derivative lignin extracted with fewer nitric acid present. The amount of total phenolics present in these derivatives are good for making antiseptics, detergents, nylon, resin and many industrial products.

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Lignin, waste, precipitation, phenols, antioxidants

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Author Biographies

María José López Villalobos, Mediwork Servicios C.A

Licenciada en Bioanálisis

Irama Isabel Piña Sáenz, Universidad del Zulia, Venezuela

Universidad del Zulia, Facultad de Ingeniería, Maracaibo, Venezuela
Doctora en Química
Correo: ipina@fing.luz.edu.ve

Yakelin Abou Masoud, Laboratorio Clinico Bonaiuto, Venezuela

Licenciada en Bioanálisis

Fredy José Ysambertt, Universidad del Zulia, Venezuela

Universidad del Zulia, Venezuela
Doctor en Química

Publicaciones en Ciencias y Tecnologia

Published

2018-06-28

How to Cite

[1]
M. J. López Villalobos, I. I. Piña Sáenz, Y. Abou Masoud, and F. J. Ysambertt, “Determination of total phenol derivatives obtained from lignin black liquor as alternative to production”, Publ.Cienc.Tecnol, vol. 9, no. 1, pp. 47-62, Jun. 2018.

Issue

Vol. 9 No. 1 (2015): January-June

Section

Research Article

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